DSpace Repository

Solid phase extraction method for the determination of iron, lead and chromium by atomic absorption spectrometry using Amberite XAD-2000 column in various water samples

Show simple item record

dc.contributor.author Elci, L.
dc.contributor.author Kartal, A.A.
dc.contributor.author Soylak, M.
dc.date.accessioned 2019-08-16T12:17:04Z
dc.date.available 2019-08-16T12:17:04Z
dc.date.issued 2008
dc.identifier.issn 03043894 (ISSN)
dc.identifier.uri http://acikerisim.pau.edu.tr:8080/xmlui/handle/11499/7172
dc.description.abstract This work describes a procedure for the separation-preconcentration of Fe(III), Pb(II) and Cr(III) from some water samples using a column-filled Amberlite XAD-2000 resin. The analyte ions retained on the column were eluted with 0.5 mol L-1 HNO3. The analytes in the effluent were determined by atomic absorption spectrometry. Several parameters governing the efficiency of the method were evaluated including pH, resin amount, sample volume, flow rates, eluent type and divers ion effects. The recoveries under the optimum working conditions were found to be as 100 ± 1% Fe, 96 ± 1% Pb and 93 ± 2% Cr. The relative standard deviations and errors were less than 2% and 5%, respectively. The detection limit based on three standard deviations of the blank was found to be 0.32, 0.51 and 0.81 μg L-1, for Fe, Pb and Cr, respectively. The procedure was applied to the determination of Fe, Cr and Pb in hot spring water and drinking water samples. © 2007 Elsevier B.V. All rights reserved.
dc.language.iso English
dc.relation.isversionof 10.1016/j.jhazmat.2007.08.075
dc.subject Chromium
dc.subject Hydroxide
dc.subject Iron
dc.subject Lead
dc.subject Preconcentration
dc.subject Solid phase
dc.subject Extraction
dc.subject Water analysis
dc.subject chromium
dc.subject drinking water
dc.subject iron
dc.subject lead
dc.subject resin
dc.subject atomic absorption spectroscopy
dc.subject extraction method
dc.subject hydroxide
dc.subject sampling
dc.subject spring water
dc.subject article
dc.subject atomic absorption spectrometry
dc.subject elution
dc.subject flow rate
dc.subject pH
dc.subject solid phase extraction
dc.subject thermal spring
dc.subject validation study
dc.subject water sampling
dc.subject Hot Springs
dc.subject Resins, Synthetic
dc.subject Solid Phase Extraction
dc.subject Spectrophotometry, Atomic
dc.subject Water Pollutants, Chemical
dc.subject Water Supply
dc.title Solid phase extraction method for the determination of iron, lead and chromium by atomic absorption spectrometry using Amberite XAD-2000 column in various water samples
dc.type Article
dc.relation.journal Journal of Hazardous Materials
dc.identifier.volume 153
dc.identifier.issue 1-2
dc.identifier.startpage 454
dc.identifier.endpage 461
dc.identifier.index Scopus


Files in this item

Files Size Format View

There are no files associated with this item.

This item appears in the following Collection(s)

Show simple item record