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Preconcentration and separation with Amberlite XAD-4 resin; determination of Cu, Fe, Pb, Ni, Cd and Bi at trace levels in waste water samples by flame atomic absorption spectrometry

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dc.contributor.author Uzun, A.
dc.contributor.author Soylak, M.
dc.contributor.author Elçi, L.
dc.date.accessioned 2019-08-16T11:47:45Z
dc.date.available 2019-08-16T11:47:45Z
dc.date.issued 2001
dc.identifier.issn 00399140 (ISSN)
dc.identifier.uri http://acikerisim.pau.edu.tr:8080/xmlui/handle/11499/5476
dc.description.abstract A method for the preconcentration of Cu, Fe, Pb, Ni, Cd and Bi as their diethyldithiocarbamate chelates was proposed using a column filled with Amberlite XAD-4 resin. The retained analytes on the resin were recovered with a small volume of acetone. The metal ions in the effluent were determined by a flame atomic absorption spectrometer. Different factors including pH of sample solution, sample volume, amount of XAD-4 resin, amount of ligand, eluent volume and matrix effects for preconcentration were examined. The recoveries for the analytes under the optimum working conditions were higher than 95%. The relative standard deviations of the determinations were below 9%. The limits of detection (3 s, n = 20) for analytes were found to be between 4 and 23 μg 1-1. The proposed method was applied to the analysis of some waste waters from the organized industrial region of Kayseri. © 2001 Elsevier Science B.V.
dc.language.iso English
dc.publisher Elsevier
dc.relation.isversionof 10.1016/S0039-9140(00)00669-X
dc.subject Metal ions
dc.subject Preconcentration
dc.subject Waste water
dc.subject XAD-4
dc.subject acetone
dc.subject bismuth
dc.subject cadmium
dc.subject chelate
dc.subject copper
dc.subject diethyldithiocarbamic acid
dc.subject iron
dc.subject lead
dc.subject ligand
dc.subject metal ion
dc.subject nickel
dc.subject polacrilin
dc.subject resin
dc.subject trace element
dc.subject analytic method
dc.subject article
dc.subject atomic absorption spectrometry
dc.subject chelation
dc.subject effluent
dc.subject pH measurement
dc.subject Turkey (republic)
dc.subject waste water
dc.title Preconcentration and separation with Amberlite XAD-4 resin; determination of Cu, Fe, Pb, Ni, Cd and Bi at trace levels in waste water samples by flame atomic absorption spectrometry
dc.type Article
dc.relation.journal Talanta
dc.identifier.volume 54
dc.identifier.issue 1
dc.identifier.startpage 197
dc.identifier.endpage 202
dc.identifier.index Scopus


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