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Solid-phase extraction of Fe(III), Pb(II) and Cr(III) in environmental samples on amberlite XAD-7 and their determinations by flame atomic absorption spectrometry

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dc.contributor.author Divrikli, Ümit.
dc.contributor.author Akdoğan, Abdullah.
dc.contributor.author Soylak, M.
dc.contributor.author Elci, Latif.
dc.date.accessioned 2019-08-16T11:32:21Z
dc.date.available 2019-08-16T11:32:21Z
dc.date.issued 2007
dc.identifier.issn 03043894 (ISSN)
dc.identifier.uri http://acikerisim.pau.edu.tr:8080/xmlui/handle/11499/4127
dc.description.abstract This paper describes a simple and accurate procedure for preconcentration of trace amounts of Fe(III), Pb(II) and Cr(III) ions. The preconcentration procedure is based on retention of p-xylenol blue chelates on Amberlite XAD-7. The analytes retained were eluted from Amberlite XAD-7 by using 1 mol L-1 HCl. The influences of the analytical parameters including amounts of reagents, pH and type of eluent were also investigated. The detection limits of Fe, Pb and Cr were found to be 3.07, 18.6 and 3.27 μg L-1, respectively. The accuracy of the procedure was checked by the analysis of an electrolytic copper wire sample. The relative error was less than 5%. The presented method was applied to the determination of Fe(III), Pb(II) and Cr(III) in water samples from Denizli, Turkey with good results such as recoveries more than 95%, relative standard deviations below 10%. © 2007 Elsevier B.V. All rights reserved.
dc.language.iso English
dc.relation.isversionof 10.1016/j.jhazmat.2007.03.084
dc.rights info:eu-repo/semantics/closedAccess
dc.subject Amberlite XAD-7
dc.subject Atomic absorption spectrometry
dc.subject p-Xylenol blue
dc.subject Preconcentration
dc.subject Electrolytic analysis
dc.subject Error analysis
dc.subject Heavy metals
dc.subject Parameter estimation
dc.subject pH effects
dc.subject Trace elements
dc.subject Water analysis
dc.subject Phase separation
dc.subject 4 xylenolsulfonphthalein
dc.subject chromium
dc.subject copper
dc.subject ferric ion
dc.subject hydrochloric acid
dc.subject lead
dc.subject phthalein
dc.subject polacrilin
dc.subject reagent
dc.subject sea water
dc.subject unclassified drug
dc.subject atomic absorption spectroscopy
dc.subject chelation
dc.subject concentration (composition)
dc.subject heavy metal
dc.subject pH
dc.subject accuracy
dc.subject article
dc.subject atomic absorption spectrometry
dc.subject electrolysis
dc.subject elution
dc.subject environmental monitoring
dc.subject flame photometry
dc.subject flow rate
dc.subject intermethod comparison
dc.subject pH measurement
dc.subject solid phase extraction
dc.subject Turkey (republic)
dc.subject water sampling
dc.subject Acrylic Resins
dc.subject Chromium
dc.subject Coloring Agents
dc.subject Electrolytes
dc.subject Hydrogen-Ion Concentration
dc.subject Ions
dc.subject Iron
dc.subject Lead
dc.subject Oceans and Seas
dc.subject Polystyrenes
dc.subject Solid Phase Extraction
dc.subject Solutions
dc.subject Spectrophotometry, Atomic
dc.subject Water
dc.subject Xylenes
dc.subject Denizli [Turkey]
dc.subject Eurasia
dc.subject Turkey
dc.title Solid-phase extraction of Fe(III), Pb(II) and Cr(III) in environmental samples on amberlite XAD-7 and their determinations by flame atomic absorption spectrometry
dc.type Article
dc.relation.journal Journal of Hazardous Materials
dc.contributor.authorID 0000-0002-7120-4380
dc.identifier.volume 149
dc.identifier.issue 2
dc.identifier.startpage 331
dc.identifier.endpage 337
dc.relation.publicationCategory Uluslararası Hakemli Dergi
dc.identifier.index Scopus
dc.identifier.index WOS
dc.identifier.index PubMed


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