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Determination of Pesticides in Soil by Mechanical Stirring-Assisted

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dc.contributor.author Akdogan, A
dc.contributor.author Kartal, AA
dc.contributor.author Hol, A
dc.contributor.author Yilmaz, Y
dc.contributor.author Divrikli, U
dc.contributor.author Elci, L
dc.date.accessioned 2019-08-20T06:36:45Z
dc.date.available 2019-08-20T06:36:45Z
dc.date.issued 2014
dc.identifier.issn 0003-2719
dc.identifier.uri http://acikerisim.pau.edu.tr:8080/xmlui/handle/11499/21953
dc.description.abstract This work describes the development of an analytical method for determining the mobility of some organophosphorus and azole group pesticides. The chromatographic and mass spectrophotometric parameters were optimized. The target pesticides were recovered quantitatively (79.3-95.6%) with a relative standard deviation less than 8.5% at the optimum conditions of the extraction. The limits of detection of the target pesticides were found to be in the range of 0.16 to 1 . 14 mu g kg (- 1 ) with a correlation coefficient ( r)> 0 . 9955 . The method was validated in the target environmental matrices by the analysis of a spiked soil sample. The proposed method was successfully applied for the determination of pesticides in vineyard soil samples and statistically evaluated.
dc.language.iso English
dc.publisher TAYLOR & FRANCIS INC
dc.relation.isversionof 10.1080/00032719.2013.845901
dc.subject Soil; Fungicide; Herbicide; Mechanical stirring-assisted extraction
dc.subject (MSAE); GC-MS
dc.title Determination of Pesticides in Soil by Mechanical Stirring-Assisted
dc.title Extraction Coupled with Gas Chromatography-Mass Spectrometry
dc.type Article
dc.relation.journal ANALYTICAL LETTERS
dc.identifier.volume 47
dc.identifier.issue 4
dc.identifier.startpage 675
dc.identifier.endpage 688
dc.identifier.index WOS


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