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Speciation of Cr(III) and Cr(VI) after column solid phase extraction on

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dc.contributor.author Bulut, VN
dc.contributor.author Duran, C
dc.contributor.author Tufekci, M
dc.contributor.author Elci, L
dc.contributor.author Soylak, M
dc.date.accessioned 2019-08-19T13:16:23Z
dc.date.available 2019-08-19T13:16:23Z
dc.date.issued 2007
dc.identifier.issn 0304-3894
dc.identifier.issn J9 J HAZARD MATER
dc.identifier.uri http://acikerisim.pau.edu.tr:8080/xmlui/handle/11499/18958
dc.description.abstract A speciation procedure for Cr(III) and Cr(VI) based on column solid phase extraction on Amberlite XAD-2010 and flame atomic absorption spectrometry combination. Cr(VI) was quantitatively recovered on Amberlite XAD-2010 resin at pH range of 2.0-3.0 as its diethyldithiocarbamate complex, while the recoveries of Cr(III) was below 5%. The influences of the various parameters including amounts of the reagents, eluent type and its volume, sample volume, etc., on the quantitative recoveries were examined. The interference of matrix and coexistent elements for method were studied. The detection limit (corresponding to three times the standard deviation of the blank) and the enrichment factor for Cr(VI) were found to be 1.28 mu g/L and 25, respectively. To verify the accuracy of the method, drinking water certified reference material (CRM-TMDW-500) was analyzed and the results obtained were in good agreement with the certified value. The proposed method has been successfully applied to the speciation of Cr(III) and Cr(VI) in water samples and preconcentration of total chromium in environmental samples. (C) 2006 Elsevier B.V. All rights reserved.
dc.language.iso English
dc.publisher ELSEVIER SCIENCE BV
dc.relation.isversionof 10.1016/j.jhazmat.2006.08.074
dc.subject speciation; chromium; solid-phase extraction; amberlite XAD-2010; atomic
dc.subject absorption spectrometry
dc.title Speciation of Cr(III) and Cr(VI) after column solid phase extraction on
dc.title Amberlite XAD-2010
dc.type Article
dc.relation.journal JOURNAL OF HAZARDOUS MATERIALS
dc.identifier.volume 143
dc.identifier.issue 1-2
dc.identifier.startpage 112
dc.identifier.endpage 117
dc.identifier.index WOS


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